Determination of total ionic alkyllead in water by electrothermal atomisation atomic absorption spectrometry

Literature Information

Publication Date
DOI 10.1039/JA9860100293
Impact Factor 4.023
Authors


View Original

Abstract

Ionic alkyllead compounds are extracted from water into carbon tetrachloride by complexation with sodium diethyldithiocarbamate while inorganic lead is effectively removed through the application of EDTA. Evaporation of the organic solvent followed by digestion of the organolead complexes with nitric acid allows the determination of the sum of the ionic alkyllead compounds by graphite furnace atomic absorption spectrometry with an over-all recovery of 85 ± 6% and a detection limit of a few ng l–1.

Related Literature

A cationic 24-MC-8 manganese cluster with ring metals possessing three oxidation states [MnII4MnIII6MnIV2(μ4-O)2(μ3-O)4(μ3-OH)4(μ3-OCH3)2(pko)12](OH)(ClO4)3‡

Catherine Dendrinou-Samara, Curtis M. Zaleski, Andri Evagorou, Jeff W. Kampf, Vincent L. Pecoraro, Dimitris P. Kessissoglou

2003-09-30 Communication

DOI: 10.1039/B309439A

Heteropoly acid as a novel nitrene transfer agent: a facile and practical aziridination of olefins with Chloramine-T

G. D. Kishore Kumar, Sundarababu Baskaran

2004-03-23 Communication

DOI: 10.1039/B402371D

Rotavap simulation and the estimation of boiling points

Craig R. Stewart, Jonathan M. Goodman

2003-09-29 Communication

DOI: 10.1039/B309488J

Unusual reactions of N-allylic difluoroenamines under thermal conditions

Hideki Amii, Yutaka Ichihara, Takashi Nakagawa, Takeshi Kobayashi, Kenji Uneyama

2003-10-20 Communication

DOI: 10.1039/B309696C

Fluorescence studies of protein thermostability in ionic liquids

Sheila N. Baker, T. Mark McCleskey, Siddharth Pandey, Gary A. Baker

2004-03-19 Communication

DOI: 10.1039/B401304M

Peptide-coated CdS quantum dots for the optical detection of copper(ii) and silver(i)‡

Kerim M. Gattás-Asfura, Roger M. Leblanc

2003-09-25 Communication

DOI: 10.1039/B308991F

Carbonate and oxalate dianions as prolific hydrogen-bond acceptors in supramolecular assembly‡

Chi-Keung Lam, Thomas C. W. Mak

2003-10-08 Communication

DOI: 10.1039/B306649E

Manganese N-confused porphyrin reactivity: CH bond activation and meso carbon reduction

John D. Harvey, Christopher J. Ziegler

2003-10-22 Communication

DOI: 10.1039/B310522A

You might also like

Compound Q&A

What is the market or research trend for N-(4-Methoxybenzyl)-2-pyridinamine (CAS: 52818-63-0)?

N-(4-Methoxybenzyl)-2-pyridinamine (CAS: 52818-63-0) is increasingly being used ...

52818-63-0N-(4-Methoxybenzyl)-...
Compound Q&A

What precautions should be taken when handling Ethyl 4-(2-chlorophenyl)-1,3-thiazole-2-carboxylate (CAS: 1050507-06-6)?

When handling Ethyl 4-(2-chlorophenyl)-1,3-thiazole-2-carboxylate, appropriate p...

1050507-06-6Ethyl 4-(2-chlorophe...
Compound Q&A

What regulatory guidelines apply to diethyldiselane (CAS: 628-39-7)?

Diethyldiselane (CAS: 628-39-7) is classified under the Globally Harmonized Syst...

628-39-7Diethyldiselane
Compound Q&A

What is the market or research trend for oxocopper (CAS: 12053-18-8)?

The market for oxocopper (CAS: 12053-18-8) is primarily driven by its use in cat...

12053-18-8oxocopper; oxo-(oxoc...
Compound Q&A

What is the market or research trend for 5-{[(2-Methyl-2-propanyl)oxy]carbonyl}-5-azaspiro[2.4]heptane-7-carboxylic acid?

The market for 5-{[(2-Methyl-2-propanyl)oxy]carbonyl}-5-azaspiro[2.4]heptane-7-c...

1268519-54-55-{[(2-Methyl-2-prop...
Compound Q&A

What is 2-(1-Pyrrolidinyl)-4-pyridinamine (CAS: 35981-63-6)?

2-(1-Pyrrolidinyl)-4-pyridinamine is a chemical compound with the CAS number 359...

35981-63-62-(1-Pyrrolidinyl)-4...
Compound Q&A

What are the physical and chemical properties of 2-(3-Pyridinyl)-1-azabicyclo[2.2.2]octane (CAS: 91556-75-1)?

2-(3-Pyridinyl)-1-azabicyclo[2.2.2]octane (CAS: 91556-75-1) is a crystalline sol...

91556-75-12-(3-Pyridinyl)-1-az...
Compound Q&A

How is (S)-Alpha-allyl-proline hydrochloride (CAS: 129704-91-2) typically synthesized?

(S)-Alpha-allyl-proline hydrochloride is usually synthesized via a Wittig reacti...

129704-91-2(S)-Alpha-allyl-prol...
Compound Q&A

What is 3-Methyl-1,2-oxazole-5-carboxylic acid (CAS: 4857-42-5)?

3-Methyl-1,2-oxazole-5-carboxylic acid (CAS: 4857-42-5) is an organic compound w...

4857-42-53-Methyl-1,2-oxazole...
Compound Q&A

How is Lys-SMCC-DM1 (CAS: 1281816-04-3) typically synthesized?

Lys-SMCC-DM1 is synthesized via a multi-step process involving the coupling of S...

1281816-04-3Lys-SMCC-DM1

Source Journal

Journal of Analytical Atomic Spectrometry

Journal of Analytical Atomic Spectrometry
CiteScore: 6.2
Self-citation Rate: 25.8%
Articles per Year: 254

The Journal of Analytical Atomic Spectrometry (JAAS) is the central journal for publishing innovative research on fundamentals, instrumentation, and methods in the determination, speciation and isotopic analysis of (trace) elements within all fields of application. This includes, but is not restricted to, the most recent progress, developments and achievements in all forms of atomic and elemental detection, isotope ratio determination, molecular analysis, plasma-based analysis and X-ray techniques. The journal welcomes full papers, communications, technical notes, critical and tutorial review articles, editorials, and comments, in addition to the Atomic Spectrometry Updates (ASU) literature reviews that are prepared by an expert panel. Submissions are welcome in the following areas, but note this list reflects the current scope and authors are strongly encouraged to contact the Editorial team if they believe that their work offers potentially new and emerging research relevant to the journal remit: Fundamental studies in the following. New and existing sources for atomic emission, absorption, fluorescence and mass spectrometry and those that provide both atomic and molecular information Sample introduction techniques for solids, liquids, gases Improvements in sensitivity, selectivity, precision, accuracy and/or robustness Isotope ratio measurements, including techniques for improving precision and mass bias correction Single channel and multichannel simultaneous detection systems Chemometrics, statistics, calibration techniques and internal standardisation Theoretical and numerical modelling of fundamental processes related to all of the above methodologies Novel or improved methodologies in areas of application including, but not limited to the following. Biosciences, including elemental, speciation and isotopic analysis in biological systems, immunoassays based on metal-labeled antibodies, bio-imaging, and nanoparticle toxicology Geochemistry Environmental science Materials science, including engineered nanoparticles and quantum dots Metrology, including reference materials Forensic analysis Food and agricultural sciences Energy Archaeometry Molecular analysis. Molecular sources for elemental and isotopic analysis Atomic sources for molecular analysis Atomic and molecular techniques simultaneously used for complementary chemical information All contributions are judged on originality and quality of scientific content, and appropriateness of length to content of new science.

Recommended Compounds

Recommended Suppliers

Disclaimer
This page provides academic journal information for reference and research purposes only. We are not affiliated with any journal publishers and do not handle publication submissions. For publication-related inquiries, please contact the respective journal publishers directly.
If you notice any inaccuracies in the information displayed, please contact us at support@chemtradehub.com. We will promptly review and address your concerns.