Intact NMR spectroscopy: slow high-resolution magic angle spinning chemical shift imaging
Literature Information
Publication Date
2020-03-04
DOI
10.1039/D0AN00118J
Impact Factor
4.616
Authors
Covadonga Lucas-Torres, Alan Wong
View Original
Abstract
High-Resolution Magic-Angle Spinning Chemical Shift Imaging (HR-MAS CSI) has recently been explored for nuclear magnetic resonance (NMR) metabolomics and shows considerable promise in organism research. This is due to its ability to offer a supplemental dimension – spatial metabolic distribution – for profiling. However, HR-MAS CSI suffers from the large centrifugal stress exerted on the sample, which inevitably hinders the metabolic assessment. Herein, a slow sample spinning strategy was implemented and evaluated. The results demonstrate its potential as a highly informative profiling approach for intact specimens, with high quality data and feasibility.
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Analyst
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Recommended Compounds
![Ethyl 2-[(3-bromo-4-pyridinyl)sulfanyl]-2-methylpropanoate structure](https://static.chemtradehub.com/structs/135/1352794-86-5-a8aa.webp "Ethyl 2-[(3-bromo-4-pyridinyl)sulfanyl]-2-methylpropanoate structure")
Ethyl 2-[(3-bromo-4-pyridinyl)sulfanyl]-2-methylpropanoate
CAS Number:
1352794-86-5
Molecular Formula:
C11H14BrNO2S
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