![5-Methoxy-1H-pyrrolo[3,2-b]pyridine structure](https://static.chemtradehub.com/structs/172/17288-40-3-a8d1.webp "5-Methoxy-1H-pyrrolo[3,2-b]pyridine structure")
Synthesis and characterization of birch wood xylan succinoylated in 1-n-butyl-3-methylimidazolium chloride
Literature Information
Publication Date
2011-06-28
DOI
10.1039/C1PY00086A
Impact Factor
5.582
Authors
Natanya M. L. Hansen, David Plackett
View Original
Abstract
The chemical modification of birch wood xylan was undertaken in the ionic liquid 1-n-butyl-3-methylimidazolium chloride (C4mimCl) using three different long-chain succinic anhydrides: n-octenyl succinic anhydride (n-OSA), n-dodecenyl succinic anhydride (n-DDSA) and n-octadecenyl succinic anhydride (n-ODSA). Reactions were performed at temperatures of 80–100 °C and reaction times of 0.5–22 hours resulting in a degree of substitution (DS) of 0.08–0.27. The formation of the desired products was confirmed through the use of 1H NMR and FT-IR, while DS was determined by titration. Thermogravimetric analysis of the modified and native xylans showed a slight lowering of thermal stability with functionalization. Contact angle measurements on spin-coated surfaces of modified xylan films showed a significant increase in hydrophobicity with the introduction of the alkenyl-functionalized succinic anhydride moieties.
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Source Journal
Polymer Chemistry
CiteScore:
8.6
Self-citation Rate:
7.3%
Articles per Year:
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Recommended Compounds
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Molecular Formula:
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Molecular Formula:
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