Facile synthesis of multi-block copolymers containing poly(ester–amide) segments with an ordered side group sequence
Literature Information
Publication Date
2013-05-08
DOI
10.1039/C3PY00382E
Impact Factor
5.582
Authors
An Lv, Xin-Xing Deng, Lei Li, Zi-Long Li, Yao-Zong Wang, Fu-Sheng Du, Zi-Chen Li
View Original
Abstract
We report a facile method for the synthesis of multi-block copolymers consisting of poly(ethylene glycol) (PEG) and poly(ester–amide) segments with an ordered side group sequence via multicomponent polymerization based on the Passerini reaction (PR). The technique involves the polymer supported liquid-phase synthesis of three PEG diacid macromonomers (M1–M3) via stepwise PR with tert-butyl isocyanoacetate and a functional aldehyde followed by selective hydrolysis, and the final multicomponent polymerization of M1–M3 with phenylacetaldehyde and 1,6-diisocyanohexane.
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Source Journal
Polymer Chemistry
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