A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS
Literature Information
Jean-Paul Amoureux, Alexandrine Flambard, Laurent Delevoye, Lionel Montagne
We show that by combining the intrinsically larger (with respect to MQMAS) efficiency of Double-Quantum Filtered Satellite-Transition MAS (DQF-STMAS), with the large S/N gain of the Soft-Pulse Added Mixing (SPAM) concept, a new very sensitive high-resolution solid-state NMR method can be obtained for semi-integer quadrupolar nuclei.
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