Photocatalytic decarboxylative phosphorylation of N-aryl glycines
Literature Information
Publication Date
2023-12-05
DOI
10.1039/D3QO01577G
Impact Factor
5.281
Authors
Jiangwei Wen, Xue Sun, Kelu Yan, Tingtao Yan, Zhen Liu, Yang Li, Jianjing Yang
View Original
Abstract
The direct decarboxylative phosphorylation of N-aryl glycines is an appealing method for the synthesis of α-amino phosphine oxides. In this study, we present the first instance of a straightforward and practical approach for achieving decarboxylative phosphorylation of N-aryl glycines to obtain α-amino phosphine oxides under visible-light photoredox catalysis. This simple visible light catalytic protocol demonstrated smooth efficiency and excellent tolerance towards functional groups. Furthermore, it can be easily scaled up to the gram scale using extremely mild conditions, all while avoiding the use of a metal and base.
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Source Journal
Organic Chemistry Frontiers
CiteScore:
7.8
Self-citation Rate:
8.7%
Articles per Year:
724
Organic Chemistry Frontiers publishes high-quality research from across organic chemistry. Emphases are placed on studies that make significant contributions to the field of organic chemistry by reporting either new or significantly improved protocols or methodologies. Topics include, but are not limited to the following: Organic synthesis Development of synthetic methodologies Catalysis Natural products Functional organic materials Supramolecular and macromolecular chemistry Physical and computational organic chemistry
Recommended Compounds
N1,N1-Bis(4-aminophenyl)benzene-1,4-diamine trihydrochloride
CAS Number:
114254-48-7
Molecular Formula:
C18H21Cl3N4
![4-Chloro-2-{[(2-chlorophenoxy)acetyl]amino}benzoic acid structure](https://static.chemtradehub.com/structs/351/351424-20-9-9467.webp "4-Chloro-2-{[(2-chlorophenoxy)acetyl]amino}benzoic acid structure")
4-Chloro-2-{[(2-chlorophenoxy)acetyl]amino}benzoic acid
CAS Number:
351424-20-9
Molecular Formula:
C15H11Cl2NO4
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