Compound Q&A

How is (2'-Amino-2-biphenylyl)(methanesulfonato-kappaO)palladium - 2'-(dicyclohexylphosphino)-N,N,N',N'-tetramethyl-2,6-biphenyldiamine (CAS: 1447963-73-6) typically synthesized?

Answer

(2'-Amino-2-biphenylyl)(methanesulfonato-kappaO)palladium - 2'-(dicyclohexylphosphino)-N,N,N',N'-tetramethyl-2,6-biphenyldiamine (1:1)
This complex is synthesized through the reaction of palladium(II) acetate with 2-(dicyclohexylphosphino)-N,N,N',N'-tetramethyl-2,6-biphenyldiamine and methanesulfonic acid. The reaction is typically performed under an inert atmosphere to prevent the palladium from oxidizing. The yield is generally around 80%, and the product is isolated by column chromatography.

About

English Name (2'-Amino-2-biphenylyl)(methanesulfonato-kappaO)palladium - 2'-(dicyclohexylphosphino)-N,N,N',N'-tetramethyl-2,6-biphenyldiamine (1:1)
Molecular Formula C41H54N3O3PPdS
Molecular Weight 806.36 g/mol
SMILES CN(C)c1cccc(c1c2ccccc2P(C3CCCCC3)C4CCCCC4)N(C)C.CS(=O)(=O)O[Pd]c1ccccc1c2ccccc2N
InChIKey SMFSVINURNWOPR-UHFFFAOYSA-M
Last Updated: 2025-10-29 13:16

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