ATRP mediated encapsulation of Gibbsite: fixation of the morphology by using a cross-linker
Literature Information
Publication Date
2017-04-24
DOI
10.1039/C7PY00226B
Impact Factor
5.582
Authors
Olessya P. Loiko, Anne B. Spoelstra, Jan Meuldijk, Johan P. A. Heuts
View Original
Abstract
Using ethylene glycol dimethacrylate (EGDMA) as a cross-linker Gibbsite platelets were successfully encapsulated fully using an ATRP-mediated emulsion polymerisation technique. Previously we reported a “muffin-like” morphology, which was obtained using the same approach without a cross-linker. This morphology was attributed to the mobility of the growing polymeric chains, allowing them to move one side of the platelet during the reaction. The addition of EGDMA reduces this mobility and it is shown that this approach indeed leads to encapsulated Gibbsite. A comprehensive study of the reaction conditions, in particular the cross-linker addition profile and concentration, was carried out in combination with cryo-TEM characterization of the final particle morphology.
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Source Journal
Polymer Chemistry
CiteScore:
8.6
Self-citation Rate:
7.3%
Articles per Year:
457
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tert-butyl 8-benzyl-2,8-diazaspiro[4.5]decane-2-carboxylate
CAS Number:
336191-16-3
Molecular Formula:
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