A study of separation selectivity using embedded ester-bonded stationary phases for liquid chromatography
Literature Information
Publication Date
2016-04-27
DOI
10.1039/C6AN00139D
Impact Factor
4.616
Authors
Szymon Bocian, Katarzyna Krzemińska, Bogusław Buszewski
View Original
Abstract
A new type of stationary bonded phase for liquid chromatography with various functional groups bonded to diol-modified silica via ester bond was synthesized. The structures of the proposed stationary phases contain: alkyl chains (C10, C18), phenyl, and cholesterol groups. The structures of the synthesized materials were confirmed by different physico-chemical techniques such as elemental analysis, infrared spectroscopy (FTIR), 13C CP/MAS NMR and liquid chromatography under reversed phase conditions (RP) and with hydrophilic interaction liquid chromatography (HILIC). Depending on the type of functionalities bonded to the Diol-Ester, the stationary phases are capable of separating various groups of compounds in RP and HILC, even using pure water as a mobile phase.
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