High temperature liquid chromatography with monolithic capillary columns and pure watereluent

Literature Information

Publication Date 2008-12-24
DOI 10.1039/B815886J
Impact Factor 4.616
Authors

Tim J. Causon, Robert A. Shellie, Emily F. Hilder


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Abstract

Use of an organic polymeric monolithic stationary phase for high temperature liquid chromatography (HTLC) with a pure water eluent is demonstrated for the first time. Separations of n-alcohols at temperatures exceeding 200 째C were achieved with no statistically significant reduction in chromatographic performance evident after continuous operation for 1000 column volumes above 200 째C.

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