Oxalic acid compound with cyclohexylsulfamothioic O-acid (11)
CAS Number:
31895-22-4
Molecular Formula:
C7H13NO4S3
Cu-catalyzed one-pot synthesis of fused oxazepinone derivatives via sp2 C–H and O–H cross-dehydrogenative coupling
Literature Information
Publication Date
2016-04-19
DOI
10.1039/C6QO00040A
Impact Factor
5.281
Authors
Zeyuan Zhang, Zhen Dai, Xinkun Ma, Yihan Liu, Xiaojun Ma, Wanli Li
View Original
Abstract
An efficient Cu-catalyzed cascade reaction protocol was developed for the synthesis of fused oxazepinone derivatives via sp2 C–H and O–H cross-dehydrogenative coupling. A readily available catalyst, Cu2O, was used in this modular and convergent approach. An unusual Smiles rearrangement reaction was involved in this synthesis. Various reaction parameters were evaluated and optimized, and the target compounds were obtained in good-to-excellent yields.
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Source Journal
Organic Chemistry Frontiers
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7.8
Self-citation Rate:
8.7%
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724
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