Microwave effect on the surface composition of the Urushibara Ni hydrogenation catalyst and improved reduction of acetophenone
Literature Information
Junichi Tsuzuki, Futoshi Sakai, Masatsugu Kajitani, Nick Serpone
The Urushibara Ni (U-Ni) hydrogenation catalyst and some modified forms, and for comparison Raney-Ni, were subjected to conventional (oil bath) and MW heating, and subsequently characterized by electron dispersive X-ray analysis (EDX), by BET surface area, and by scanning electron microscopy (SEM); yields of the catalyzed hydrogenation of acetophenone to 1-phenylethanol in 2-propanol by one of the modified forms (U-Ni-B) were greatly improved (from 68% to 95%).
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