4-(Dibenzylamino)tetrahydro-2H-pyran-4-carbonitrile
CAS Number:
1630906-81-8
Molecular Formula:
C20H22N2O
A reductive recycle strategy for the facile synthesis of molybdenum(VI) alkylidyne catalysts for alkyne metathesis
Literature Information
Publication Date
2003-02-27
DOI
10.1039/B212405J
Impact Factor
6.222
Authors
Wei Zhang, Stefan Kraft, Jeffrey S. Moore
View Original
Abstract
A convenient synthesis of trisamido molybdenum(VI) alkylidyne complexes has been developed, in which the key step is the addition of a geminal dichloride to a trisamido molybdenum(III) complex in the presence of magnesium to continuously recycle unwanted side product 4, selectively generating the desired alkylidyne complexes in high yield.
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Source Journal
Chemical Communications
CiteScore:
8.6
Self-citation Rate:
4.7%
Articles per Year:
2458
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