Compound Q&A

How is 1,2-Dimethoxy-12-methyl[1,3]benzodioxolo[5,6-c]phenanthridin-12-ium 13-methyl[1,3]benzodioxolo[5,6-c][1,3]dioxolo[4,5-i]phenanthridin-13-ium chloride (CAS: 112025-60-2) typically synthesized?

Answer

1,2-Dimethoxy-12-methyl[1,3]benzodioxolo[5,6-c]phenanthridin-12-ium 13-methyl[1,3]benzodioxolo[5,6-c][1,3]dioxolo[4,5-i]phenanthridin-13-ium chloride (1:1:2)
This compound is typically synthesized through a multi-step process involving the coupling of appropriate precursors. Commonly, it is synthesized from benzodioxolo[5,6-c]phenanthridine derivatives using palladium catalysis under microwave conditions. The reaction is known to have good selectivity and yield, with the final step involving hydrochloric acid treatment to form the chloride salt.

About

English Name 1,2-Dimethoxy-12-methyl[1,3]benzodioxolo[5,6-c]phenanthridin-12-ium 13-methyl[1,3]benzodioxolo[5,6-c][1,3]dioxolo[4,5-i]phenanthridin-13-ium chloride (1:1:2)
Molecular Formula C41H32Cl2N2O8
Molecular Weight 751.6 g/mol
SMILES C[N+]1=C2C(=C3C=CC4=C(C3=C1)OCO4)C=CC5=CC6=C(C=C52)OCO6.C[N+]1=C2C(=C3C=CC(=C(C3=C1)OC)OC)C=CC4=CC5=C(C=C42)OCO5.[Cl-].[Cl-]
InChIKey IGMMBJRQHHXEHN-UHFFFAOYSA-L
Last Updated: 2025-10-10 19:08

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