Probe design for the direct insertion of solid samples in the inductively coupled plasma for analysis by atomic emission and mass spectrometry

Literature Information

Publication Date
DOI 10.1039/JA9890400721
Impact Factor 4.023
Authors


View Original

Abstract

An alternative to the conventional probes used for the direct introduction of solid samples into the inductively coupled plasma is presented. Powdered samples have been mixed with graphite and pressed into pellets, which were then inserted into the plasma. Unlike other probes, such as graphite cups, the whole body of these pellets was composed of sample mixture, so more sample could be inserted into the plasma at once. For some elements, the resulting improvement in detection limits was commensurate with the increased mass of sample whereas for other elements it was greater, suggesting that the absence of walls on the probes may result in better heat and mass transfers.

Related Literature

Thermal transport in monocrystalline and polycrystalline lithium cobalt oxide

Jinlong He, Lin Zhang, Ling Liu

2019-05-31 Paper

DOI: 10.1039/C9CP01585J

Oxygen transport and surface exchange mechanisms in LSCrF–ScCeSZ dual-phase ceramics

Zonghao Shen, Stephen J. Skinner, John A. Kilner

2019-05-24 Paper

DOI: 10.1039/C9CP02175B

Non-adiabatic molecular dynamics investigation of the size dependence of the electronic relaxation in polyacenes

Evgeny Posenitskiy, Mathias Rapacioli, Bruno Lepetit, Didier Lemoine, Fernand Spiegelman

2019-05-17 Paper

DOI: 10.1039/C9CP00603F

Vibrational sum-frequency generation spectroscopy of electrode surfaces: studying the mechanisms of sustainable fuel generation and utilisation

Adrian M. Gardner, Khezar H. Saeed, Alexander J. Cowan

2019-05-23 Perspective

DOI: 10.1039/C9CP02225B

The performance of adsorption, dissociation and diffusion mechanism of hydrogen on the Ti-doped ZrCo(110) surface

Qingqing Wang, Xianggang Kong, Huilei Han, Ge Sang, Guanghui Zhang, Tao Gao

2019-05-15 Paper

DOI: 10.1039/C9CP02491C

Structural and functional role of anions in electrochemical water oxidation probed by arsenate incorporation into cobalt-oxide materials

Javier Villalobos, Katharina Klingan, Petko Chernev, Paul Kubella, Roberto Urcuyo, Chiara Pasquini, Rodney D. L. Smith, Mavis L. Montero, Holger Dau

2019-05-10 Paper

DOI: 10.1039/C9CP01754B

Intrinsic magnetism and biaxial strain tuning in two-dimensional metal halides V3X8 (X = F, Cl, Br, I) from first principles and Monte Carlo simulation

Haibo Xiao, Xiaonan Wang, Ruilong Wang, Lingfang Xu, Shiheng Liang, Changping Yang

2019-05-09 Paper

DOI: 10.1039/C9CP00850K

Chemical equilibria of aqueous ammonium–carboxylate systems in aqueous bulk, close to and at the water–air interface

Yina Salamanca Blanco, Önder Topel, Éva G. Bajnóczi, Olle Björneholm, Ingmar Persson

2019-05-22 Paper

DOI: 10.1039/C9CP02449B

Conformational dynamics and allosteric effect modulated by the unique zinc-binding motif in class IIa HDACs

Huawei Liu, Fan Zhang, Kai Wang, Xiaowen Tang, Ruibo Wu

2019-05-30 Paper

DOI: 10.1039/C9CP02261A

Pretransitional behavior of viscoelastic parameters at the nematic to twist-bend nematic phase transition in flexible n-mers

Zeinab Parsouzi, Mojtaba Rajabi, Rony Saha, Prabesh Gyawali, Alan R. Baldwin, Chris Welch, Georg H. Mehl, J. T. Gleeson, Samuel Sprunt

2019-05-20 Paper

DOI: 10.1039/C9CP00984A

You might also like

Compound Q&A

What are the main uses of 1H-Indazole-6-carbonitrile (CAS: 141290-59-7)?

1H-Indazole-6-carbonitrile finds applications in pharmaceuticals, where it serve...

141290-59-71H-Indazole-6-carbon...
Compound Q&A

How should waste containing Dioctyl (2E)-2-butenedioate (CAS: 2997-85-5) be handled?

Waste containing Dioctyl (2E)-2-butenedioate (CAS: 2997-85-5) should be collecte...

2997-85-5Dioctyl (2E)-2-buten...
Compound Q&A

What industries use Sodium [(1,2-benzoxazol-3-ylmethyl)sulfonyl]azanide (CAS: 68291-98-5)?

Sodium [(1,2-benzoxazol-3-ylmethyl)sulfonyl]azanide is primarily used in pharmac...

68291-98-5Sodium [(1,2-benzoxa...
Compound Q&A

Are there alternatives to Dimethyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,6-pyridinedicarboxylate (CAS: 741709-66-0) in synthesis?

Dimethyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,6-pyridinedicarboxyla...

741709-66-0Dimethyl 4-(4,4,5,5-...
Compound Q&A

How should waste containing 2-Fluoro-6-hydrazinopyridine (CAS: 80714-39-2) be handled?

Waste containing 2-Fluoro-6-hydrazinopyridine (CAS: 80714-39-2) should be manage...

80714-39-22-Fluoro-6-hydrazino...
Compound Q&A

What is 6-Formyl-2-pyridinecarboxylic acid (CAS: 499214-11-8)?

6-Formyl-2-pyridinecarboxylic acid is an organic compound with the molecular for...

499214-11-86-Formyl-2-pyridinec...
900874-91-13-(3,4-dimethoxyphen...
Compound Q&A

How is 9H-Tribenzo[b,d,f]azepine (CAS: 29875-73-8) typically synthesized?

9H-Tribenzo[b,d,f]azepine is typically synthesized via a multi-step process invo...

29875-73-89H-Tribenzo[b,d,f]az...
Compound Q&A

How is 1-Cyclopropyl-7-ethoxy-6-fluoro-8-methoxy-4-oxo-1,4-dihydro-3-quinolinecarboxylic acid (CAS: 1797982-51-4) typically synthesized?

1-Cyclopropyl-7-ethoxy-6-fluoro-8-methoxy-4-oxo-1,4-dihydro-3-quinolinecarboxyli...

1797982-51-41-Cyclopropyl-7-etho...
Compound Q&A

How should waste containing Methyl 3-oxo-1,2,3,4-tetrahydro-6-quinoxalinecarboxylate (CAS: 671820-52-3) be handled?

Waste containing Methyl 3-oxo-1,2,3,4-tetrahydro-6-quinoxalinecarboxylate (CAS: ...

671820-52-3Methyl 3-oxo-1,2,3,4...

Source Journal

Journal of Analytical Atomic Spectrometry

Journal of Analytical Atomic Spectrometry
CiteScore: 6.2
Self-citation Rate: 25.8%
Articles per Year: 254

The Journal of Analytical Atomic Spectrometry (JAAS) is the central journal for publishing innovative research on fundamentals, instrumentation, and methods in the determination, speciation and isotopic analysis of (trace) elements within all fields of application. This includes, but is not restricted to, the most recent progress, developments and achievements in all forms of atomic and elemental detection, isotope ratio determination, molecular analysis, plasma-based analysis and X-ray techniques. The journal welcomes full papers, communications, technical notes, critical and tutorial review articles, editorials, and comments, in addition to the Atomic Spectrometry Updates (ASU) literature reviews that are prepared by an expert panel. Submissions are welcome in the following areas, but note this list reflects the current scope and authors are strongly encouraged to contact the Editorial team if they believe that their work offers potentially new and emerging research relevant to the journal remit: Fundamental studies in the following. New and existing sources for atomic emission, absorption, fluorescence and mass spectrometry and those that provide both atomic and molecular information Sample introduction techniques for solids, liquids, gases Improvements in sensitivity, selectivity, precision, accuracy and/or robustness Isotope ratio measurements, including techniques for improving precision and mass bias correction Single channel and multichannel simultaneous detection systems Chemometrics, statistics, calibration techniques and internal standardisation Theoretical and numerical modelling of fundamental processes related to all of the above methodologies Novel or improved methodologies in areas of application including, but not limited to the following. Biosciences, including elemental, speciation and isotopic analysis in biological systems, immunoassays based on metal-labeled antibodies, bio-imaging, and nanoparticle toxicology Geochemistry Environmental science Materials science, including engineered nanoparticles and quantum dots Metrology, including reference materials Forensic analysis Food and agricultural sciences Energy Archaeometry Molecular analysis. Molecular sources for elemental and isotopic analysis Atomic sources for molecular analysis Atomic and molecular techniques simultaneously used for complementary chemical information All contributions are judged on originality and quality of scientific content, and appropriateness of length to content of new science.

Recommended Compounds

Recommended Suppliers

Disclaimer
This page provides academic journal information for reference and research purposes only. We are not affiliated with any journal publishers and do not handle publication submissions. For publication-related inquiries, please contact the respective journal publishers directly.
If you notice any inaccuracies in the information displayed, please contact us at support@chemtradehub.com. We will promptly review and address your concerns.