![methyl 6-amino-1H-pyrrolo[2,3-b]pyridine-4-carboxylate structure](https://static.chemtradehub.com/structs/119/1190315-60-6-9d9a.webp "methyl 6-amino-1H-pyrrolo[2,3-b]pyridine-4-carboxylate structure")
methyl 6-amino-1H-pyrrolo[2,3-b]pyridine-4-carboxylate
CAS Number:
1190315-60-6
Molecular Formula:
C9H9N3O2
Ring-opening copolymerisation of cyclohexene oxide and carbon dioxide catalysed by scorpionate zinc complexes
Literature Information
Publication Date
2016-10-04
DOI
10.1039/C6PY01559J
Impact Factor
5.582
Authors
Javier Martínez, José A. Castro-Osma, Agustín Lara-Sánchez, Antonio Otero, Juan Fernández-Baeza, Juan Tejeda, Luis F. Sánchez-Barba, Antonio Rodríguez-Diéguez
View Original
Abstract
A series of new acetate and trifluroacetate bimetallic zinc complexes containing heteroscorpionate ligands have been prepared in very high yields. The structures of the complexes were determined by spectroscopic methods, and the single-crystal X-ray structure of complex 6 confirmed a κ3-NNO coordination mode of the scorpionate ligand in a dinuclear molecular arrangement. Bimetallic zinc complexes 6–11 were investigated as catalysts for the synthesis of polycarbonates from epoxides and carbon dioxide in the absence of a cocatalyst. Under the optimal reaction conditions, complex 10 acts as an efficient single-component initiator for the ring-opening copolymerisation of cyclohexene oxide and carbon dioxide, yielding polycarbonate materials with narrow polydispersities.
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Source Journal
Polymer Chemistry
CiteScore:
8.6
Self-citation Rate:
7.3%
Articles per Year:
457
Polymer Chemistry welcomes submissions in all areas of polymer science that have a strong focus on macromolecular chemistry. Manuscripts may cover a broad range of fields, yet no direct application focus is required.
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