Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

Literature Information

Publication Date 2009-03-02
DOI 10.1039/B818867J
Impact Factor 3.676
Authors

Daniel Lee, Jochem Struppe, Douglas W. Elliott, Leonard J. Mueller, Jeremy J. Titman


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Abstract

A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50%-U-13C-CsC60.

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Physical Chemistry Chemical Physics

Physical Chemistry Chemical Physics
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