Quantitative determination of lead in mixtures of lead(ii) halides using solid-state 207Pb NMR spectroscopy
Literature Information
Publication Date
2006-09-05
DOI
10.1039/B609870C
Impact Factor
4.616
Authors
Alicia Glatfelter, Nicole Stephenson, Shi Bai, Cecil Dybowski, Dale L. Perry
View Original
Abstract
We demonstrate a multi-spectrum technique for facile, quantitative determination of lead in solid materials using solid-state 207Pb NMR that avoids the major problem of uniform excitation across a wide spectral range; the method can be employed without chemical separation or other chemical manipulations and without any prior sample preparation, resulting in a non-destructive analysis, and producing results that are in agreement with gravimetric analyses of mixed samples of the lead halides.
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