Concomitant dimorphs of tri-O-[p-halobenzoyl]-myo-inositol 1,3,5-orthoformates with different halogen bonding contacts: first order crystal-to-crystal thermal phase transition of kinetic form to the thermodynamic form
Literature Information
Publication Date
2005-10-25
DOI
10.1039/B511754B
Impact Factor
6.222
Authors
Rajesh G. Gonnade, Mohan M. Bhadbhade, Mysore S. Shashidhar, Aditya K. Sanki
View Original
Abstract
Crystallization of tri-O-[p-halobenzoyl]-myo-inositol 1,3,5-orthoformates from ethyl acetate–petroleum ether solution produced concomitant dimorphs that have different halogen bonding contacts; the kinetic form with C–Br⋯O–C contacts upon heating to 185 °C, converts completely to the thermodynamic form with C–Br⋯OC contacts via crystal-to-crystal first order phase transition.
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