3D printed metal columns for capillary liquid chromatography

Literature Information

Publication Date 2014-09-30
DOI 10.1039/C4AN01476F
Impact Factor 4.616
Authors

S. Sandron, B. Heery, V. Gupta, D. A. Collins, E. P. Nesterenko, P. N. Nesterenko, M. Talebi, S. Beirne, F. Thompson, G. G. Wallace, D. Brabazon, F. Regan, B. Paull


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Abstract

Coiled planar capillary chromatography columns (0.9 mm I.D. × 60 cm L) were 3D printed in stainless steel (316L), and titanium (Ti–6Al–4V) alloys (external dimensions of ∼5 × 30 × 58 mm), and either slurry packed with various sized reversed-phase octadecylsilica particles, or filled with an in situ prepared methacrylate based monolith. Coiled printed columns were coupled directly with 30 × 30 mm Peltier thermoelectric direct contact heater/cooler modules. Preliminary results show the potential of using such 3D printed columns in future portable chromatographic devices.

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