Synthesis of thiophosphates through a three-component reaction by using sulfur dioxide as the sulfur source
Literature Information
Publication Date
2017-08-17
DOI
10.1039/C7QO00634A
Impact Factor
5.281
Authors
Xinxing Gong, Jiahao Chen, Jianhe Liu
View Original
Abstract
Generation of thiophosphates through a three-component reaction of diaryliodonium tetrafluoroborates, 1,4-diazabicyclo[2.2.2]octane-sulfur dioxide (DABCO·(SO2)2), and diarylphosphine oxides under visible light irradiation is described. In this transformation, sulfur dioxide acts as the sulfur source, and reduction of arylsulfonyl radicals is the key step to fulfill the thiolation with diarylphosphine oxides.
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Source Journal
Organic Chemistry Frontiers
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8.7%
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Organic Chemistry Frontiers publishes high-quality research from across organic chemistry. Emphases are placed on studies that make significant contributions to the field of organic chemistry by reporting either new or significantly improved protocols or methodologies. Topics include, but are not limited to the following: Organic synthesis Development of synthetic methodologies Catalysis Natural products Functional organic materials Supramolecular and macromolecular chemistry Physical and computational organic chemistry
Recommended Compounds
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S-[2,3-Bis(palmitoyloxy)propyl]-N-[(9H-fluoren-9-ylmethoxy)(hydroxy)methylene]cysteine
CAS Number:
210532-98-2
Molecular Formula:
C53H83NO8S
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