Palladium nanoparticles supported on a carbazole functionalized mesoporous organic polymer: synthesis and their application as efficient catalysts for the Suzuki–Miyaura cross coupling reaction
Literature Information
Publication Date
2017-01-26
DOI
10.1039/C6PY01784C
Impact Factor
5.582
Authors
Hui Zhou, Chuanguang Wu, Qiaolin Wu, Bixuan Guo, Wanting Liu, Guanghua Li, Ying Mu
View Original
Abstract
A carbazole functionalized mesoporous organic polymer (CzMOP) was synthesized by carbazolyl oxidative coupling polymerization. The nitrogen-rich CzMOP material was used as a good organic support for loading palladium nanoparticles to develop heterogeneous catalysts. The CzMOP and Pd nanoparticle supported MOP (Pd@CzMOP) was fully characterized using Brunauer–Emmett–Teller (BET) surface area analysis, X-ray diffraction analysis (XRD), Fourier transform infrared (FTIR) spectroscopy, solid-state 13C NMR spectroscopy, field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and thermogravimetric analysis (TGA). The Pd@CzMOP material exhibited excellent catalytic activity towards Suzuki–Miyaura cross coupling between aryl halides and phenyl boronic acid substrates. The catalytic system was found to be recycled up to five times without significant loss of catalytic activity.
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Source Journal
Polymer Chemistry
CiteScore:
8.6
Self-citation Rate:
7.3%
Articles per Year:
457
Polymer Chemistry welcomes submissions in all areas of polymer science that have a strong focus on macromolecular chemistry. Manuscripts may cover a broad range of fields, yet no direct application focus is required.
Recommended Compounds
![[(1S,2S,3R,4S,7R,9S,10S,12R,15S)-4,12-Diacetyloxy-15-[(2R,3S)-3-benzamido-3-phenyl-2-(2,2,2-trichloroethoxycarbonyloxy)propanoyl]oxy-1,9-dihydroxy-10,14,17,17-tetramethyl-11-oxo-6-oxatetracyclo[11.3.1.03,10.04,7]heptadec-13-en-2-yl] benzoate structure](https://static.chemtradehub.com/structs/100/100431-55-8-7104.webp "[(1S,2S,3R,4S,7R,9S,10S,12R,15S)-4,12-Diacetyloxy-15-[(2R,3S)-3-benzamido-3-phenyl-2-(2,2,2-trichloroethoxycarbonyloxy)propanoyl]oxy-1,9-dihydroxy-10,14,17,17-tetramethyl-11-oxo-6-oxatetracyclo[11.3.1.03,10.04,7]heptadec-13-en-2-yl] benzoate structure")
![1-[(4-Methylphenyl)sulfonyl]-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine-5-carbonitrile structure](https://static.chemtradehub.com/structs/143/1434747-57-5-fc0d.webp "1-[(4-Methylphenyl)sulfonyl]-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine-5-carbonitrile structure")
1-[(4-Methylphenyl)sulfonyl]-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine-5-carbonitrile
CAS Number:
1434747-57-5
Molecular Formula:
C21H22BN3O4S
2,2-dideuterio-2-(3,4,5,6-tetradeuterio-2-pyridyl)acetic acid;hydrochloride
CAS Number:
1329799-67-8
Molecular Formula:
C7H2ClD6NO2
6-CHLORO-2,3-DIOXO-1,2,3,4-TETRAHYDROQUINOXALINE, 97
CAS Number:
169-14-2
Molecular Formula:
C8H5ClN2O2
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