2,2-dideuterio-2-(3,4,5,6-tetradeuterio-2-pyridyl)acetic acid;hydrochloride
CAS Number:
1329799-67-8
Molecular Formula:
C7H2ClD6NO2
Continuous flow SET-LRP in the presence of P(VDF-co-CTFE) as macroinitiator in a copper tubular reactor
Literature Information
Publication Date
2015-11-09
DOI
10.1039/C5PY01728A
Impact Factor
5.582
Authors
Ning Zhu, Xin Hu, Yajun Zhang, Kai Zhang, Zhenjiang Li, Kai Guo
View Original
Abstract
A green, highly effective and energy-saving route to the grafting modification of polymers was developed via continuous flow single electron transfer living radical polymerization (SET-LRP) in a copper tubular reactor. Polymerizations of methyl methacrylate and acrylonitrile in the presence of poly(vinylidene fluoride-co-chlorotrifluoroethylene) as the macroinitiator were used as model investigation systems. Significant benefits were achieved in the continuous flow mode compared to a batch reactor including diminished inconsistent induction times and suppressed “hot spot” effects. Furthermore, accelerated reaction rates, lower reaction temperatures and decreased ligand feed concentrations were observed by utilizing the copper tubular reactor. The structures of the modified P(VDF-co-CTFE) graft copolymers were characterized using 1H NMR, 19F NMR, FT-IR, and SEC.
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Source Journal
Polymer Chemistry
CiteScore:
8.6
Self-citation Rate:
7.3%
Articles per Year:
457
Polymer Chemistry welcomes submissions in all areas of polymer science that have a strong focus on macromolecular chemistry. Manuscripts may cover a broad range of fields, yet no direct application focus is required.
Recommended Compounds
1,3(2H,4H)-Isoquinolinedione, 7-amino-4,4-dimethyl-
CAS Number:
14576-22-8
Molecular Formula:
C11H12N2O2
6-Bromo-3,4-dihydro-2H-1,4-benzoxazine hydrochloride (1:1)
CAS Number:
1260803-10-8
Molecular Formula:
C8H9BrClNO
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